# 1 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf" ;hmqcgpqf ;avance-version (07/04/04) ;HMQC ;2D H-1/X correlation via heteronuclear zero and double quantum ; coherence ;with decoupling during acquisition ;using gradient pulses for selection ;use pulseprogram 'hmqcgpnd1d' for setup ; ;$CLASS=HighRes ;$DIM=2D ;$TYPE= ;$SUBTYPE= ;$COMMENT= # 1 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/Avance.incl" 1 ;Avance2.incl ; for 1 ; ;avance-version (09/07/02) ; ;$CLASS=HighRes Incl ;$COMMENT= ;$Id: Avance2.incl,v 1.17.2.2 2009/11/18 11:19:58 ber Exp $ # 17 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf" 2 # 1 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/Grad.incl" 1 ;Grad2.incl - include file for Gradient Spectroscopy ; for 1 ; ;avance-version (07/01/17) ; ;$CLASS=HighRes Incl ;$COMMENT= define list EA= ;$Id: Grad2.incl,v 1.12 2007/01/22 14:22:35 ber Exp $ # 18 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf" 2 # 1 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/Delay.incl" 1 ;Delay.incl - include file for commonly used delays ; ;version 00/02/07 ; ;$CLASS=HighRes Incl ;$COMMENT= ;general delays define delay DELTA define delay DELTA1 define delay DELTA2 define delay DELTA3 define delay DELTA4 define delay DELTA5 define delay DELTA6 define delay DELTA7 define delay DELTA8 define delay TAU define delay TAU1 define delay TAU2 define delay TAU3 define delay TAU4 define delay TAU5 ;delays for centering pulses define delay CEN_HN1 define delay CEN_HN2 define delay CEN_HN3 define delay CEN_HC1 define delay CEN_HC2 define delay CEN_HC3 define delay CEN_HC4 define delay CEN_HP1 define delay CEN_HP2 define delay CEN_CN1 define delay CEN_CN2 define delay CEN_CN3 define delay CEN_CN4 define delay CEN_CP1 define delay CEN_CP2 ;loop counters define loopcounter COUNTER define loopcounter SCALEF define loopcounter FACTOR1 define loopcounter FACTOR2 define loopcounter FACTOR3 ;$Id: Delay.incl,v 1.12 2005/11/10 12:16:58 ber Exp $ # 19 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf" 2 "p2=p1*2" "d2=1s/(cnst2*2)" "d12=20u" "d13=4u" "d0=3u" "in0=inf1/2" "DELTA1=d2-p16-d16-d13-d12" # 1 "mc_line 36 file /opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf expanding definition part of mc command before ze" define delay MCWRK define delay MCREST "MCWRK = 0.500000*d1" "MCREST = d1 - d1" dccorr # 36 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf" 1 ze # 1 "mc_line 36 file /opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf expanding definition of mc command after ze" # 37 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf" # 1 "mc_line 37 file /opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf expanding start label for mc command" 2 MCWRK do:f2 LBLF1, MCWRK MCREST # 38 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf" 3 p1 ph1 d2 pl2:f2 setnmr3|0 setnmr0|34|32|33 ctrlgrad 0 p3:f2 ph3 d0 p16:gp1 d16 p2 ph2 d13 p16:gp2 d16 d0 p3:f2 ph4 d13 p16:gp3 d16 DELTA1 d12 pl12:f2 setnmr3^0 setnmr0^34^32^33 ctrlgrad 7 go=2 ph31 cpd2:f2 # 1 "mc_line 56 file /opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf expanding mc command in line" MCWRK do:f2 wr #0 if #0 zd id0 lo to LBLF1 times td1 MCWRK # 57 "/opt/topspin_2.1/exp/stan/nmr/lists/pp/hmqcgpqf" exit ph1=0 ph2=0 ph3=0 2 ph4=0 0 2 2 ph31=0 2 2 0 ;pl1 : f1 channel - power level for pulse (default) ;pl2 : f2 channel - power level for pulse (default) ;pl12: f2 channel - power level for CPD/BB decoupling ;p1 : f1 channel - 90 degree high power pulse ;p2 : f1 channel - 180 degree high power pulse ;p3 : f2 channel - 90 degree high power pulse ;p16: homospoil/gradient pulse ;d0 : incremented delay (2D) [3 usec] ;d1 : relaxation delay; 1-5 * T1 ;d2 : 1/(2J)XH ;d12: delay for power switching [20 usec] ;d13: short delay [4 usec] ;d16: delay for homospoil/gradient recovery ;cnst2: = J(XH) ;inf1: 1/SW(X) = 2 * DW(X) ;in0: 1/(2 * SW(X)) = DW(X) ;nd0: 2 ;NS: 1 * n ;DS: 16 ;td1: number of experiments ;FnMODE: QF ;cpd2: decoupling according to sequence defined by cpdprg2 ;pcpd2: f2 channel - 90 degree pulse for decoupling sequence ;use gradient ratio: gp 1 : gp 2 : gp 3 ; 50 : 30 : 40.1 for C-13 ; 70 : 30 : 50.1 for N-15 ;for z-only gradients: ;gpz1: 50% for C-13, 70% for N-15 ;gpz2: 30% ;gpz3: 40.1% for C-13, 50.1% for N-15 ;use gradient files: ;gpnam1: SINE.100 ;gpnam2: SINE.100 ;gpnam3: SINE.100 ;$Id: hmqcgpqf,v 1.4 2007/04/11 13:34:30 ber Exp $